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Laboratory of NMR Spectroscopy



Laboratory head:

(nieznane) (nieznane),

 
 

laboratory members

basic information
 

 



We have two AVANCE II spectrometers from Bruker, with proton frequencies 500 MHz and 300 MHz.

The 500 MHz spectrometer is a multi-purpose research instrument. Avance II electronics console was installed on the magnet previously part of the Bruker AMX 500.

Three liquids probes are available and one for CPMAS:

  • 5 mm TBI (1H, 13C, X) with and X,Y,Z-gradient accessories, channel 1H for observation, 13C channel and/or X for decoupling.

  • 5 mm QNP

  • 10 mm BBO

  • 4 mm CPMAS

    • The 300 MHz machine is for rutine experiments with a computer tunable (ATM) and Z-gradient 5 mm BBO probe covering 109Ag to 31P.

    LIST OF PUBLICATION DURING LAST TEN YEARS.
    1. "The Influence of some Xanthone Derivatives on the Activity of J-774A.1 Cells"
      Marona, H., Pękala, E., Gunia, A., Czuba, Z., Szneler, E., Sadowski, T., Król, W.;
      Sci Pharm. 2009; 77: 743-754
    2. "Preliminary evaluation of pharmacological properties of some xanthone derivatives"
      Marona, H., Szkaradek, N., Rapacz, A., Filipek, B., Dybała, M., Siwek, A., Cegła, M., Szneler, E.;
      Bioorganic & Medicinal Chemistry 17 (2009) 1345-1352
    3. "Antifungal and Antibacterial Activity of the Newly Synthesized 2-Xanthone Derivatives"
      Marona H., Szkaradek N., Karczewska E., Trojanowska D., Budak A., Bober P., Przepiórka W., Cegla M., and Szneler E.;
      Arch. Pharm. Chem. Life Sci. 2009, 342, 9-18
    4. "Synthesis and antimycobacterial assay of some xanthone derivatives"
      Szkaradek, N., Stachura, K., Waszkielewicz, A. M., Cegła, M., Szneler, E., Marona, H.;
      Acta Poloniae Pharmaceutica 2008; 65(1): 21-8.
    5. "Synthesis and evaluation of some xanthone derivatives for anti-arrhythmic, hypotensive properties and their affinity for adrenergic receptors."
      Marona H., Szkaradek N., Kubacka M., Bednarski M., Filipek B., Cegła M., Szneler E.
      Archiv der Pharmazie 2008; 341(2): 90-8.
    6. "Anticonvulsant activity of some xanthone derivatives"
      Marona H., Pękala E., Antkiewicz-Michaluk L., Walczak M., Szneler E.;
      Bioorganic & Medicinal Chemistry 2008; 16(15): 7234-44.
    7. "Sesquiterpenoids of Picris koreana and their chemotaxonomic significance"
      Michalska, K., Szneler, E., Kisiel, W.;
      Biochemical Systematic and Ecology, 32, (2007), 459-461
    8. "Synthesis of novel, chiral, water-soluble isothiazole derivatives"
      Cież, D., Szneler, E.;
      J. Chem. Res. 4, (2007), 200-203.
    9. "An Approach to Understand the Complexation of Supramolecular Dye Congo Red with Immunoglobulin L Chain l"
      Król, M., Roterman, I., Piekarska, B., Konieczny, L., Rybarska, J., Stopa, B., Spólnik, P., Szneler E.;
      Biopolymers, 2005, (77), 155-162
    10. "Preliminary Evaluation of Anticonvulsant Activity of some Aroxyacetamides and Aroxyethylamines"
      Marona, H., Waszkielewicz A., M., Szneler E.;
      Acta Pol. Pharm.-Drug Res., 2005, 5, (62), 345-353
    11. "Furofuran lignans from a callus culture of Cichorium intybus"
      Malarz, J., Stojakowska. A., Szneler, E., Kisiel, W.;
      Plant Cell Reports - Physiology and Biochemistry, 2005, 4, (24) 226-249
    12. "Synthesis of Optically Active Isothiazole Derivatives from L-(a)-Amino Acids"
      Cież, D., Szneler, E.;
      Monatshefte für Chemie 2005, (136), 2059-2066
    13. "Synthesis and anticonvulsant activity of some piperazine derivatives"
      Marona, H., Korona, R., Szneler, E.;
      Boll. Chim. Farmac, Anno 2004, 9, (143), 329-335
    14. "Norisoprenoids from aerial parts of Cichorium pumilium"
      Kisiel W., Michalska K., Szneler E.;
      Biochemical Systematic and Ecology, 32 (2004) 343-346
    15. "Preliminart Evaluarion of Anticonvulsant Activity of some 4-(Benzyloxy)-Benzamides"
      Marona, H., Szneler, E.;
      Acta Pol. Pharm. -Drug Res. 2003, 60 (6), 479
    16. "Synthesis of 1,4-Diazines by Ring Expansion of 1,3-Diazines
      Zaleska, B., Socha, R., Karelus, M., Szneler, E., Grochowski, J., Serda, P.;
      J. Org. Chem. 2003, 68, 2334
    17. "Sulphoacetaldehyde as a product of taurine chloramine peroxidation at site of inflammation"
      Olszowski, S., Olszowska, E., Kusior, D., Szneler, E.;
      Amino Acids 2002, 22, 145
    18. "Sesquiterpene Lactones from Crepis zacintha "
      Kisiel W., Michalska K., Szneler E.;
      Polish J. Chem, 2002, 76 ,1571
    19. "Structures and Conformations of 1-Aryl-1,4-dihydro-3(2H)isoquinolines"
      Karolak-Wojciechowska J., Czyłkowski R., Karczmarzyk Z., Paluchowska M.H., Rys B., Szneler E., Mokrosz M.J.;
      J. Molecular Structure, 2002, 612(1), 39
    20. "Heat-Inducedn Formation of a Specific Binding Site for Self-Assembled Congo Red in the V Domain of Immunoglobulin L Chain l"
      Piekarska, B., Konieczny, L., Rybarska, J., Stopa, B., Zemanek, G., Szneler, E., Król, M., Nowak, M., Roterman I.;
      Biopolymers, 2001, (59), 446
    21. "Pharmacological Properties of Some Aminoalkanolic Derivatives of Xanthone"
      Marona, H., Pękala, E., Filipek, B., Maciąg, D., Szneler E.;
      Die Pharmazie, 2001, (56), 7
    22. "A New Lupane-Type Triterpenoid from Taraxacum officinale "
      Kisiel, W., Barszcz, B., Szneler, E.;
      Polish J. Chem., 2000, (74), 281

     

    last modified: Krzysztof Szczeponek, 2010-03-21 18:34:00
    		   

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