Prof. Wacław Makowski
Department of Chemical Education
Department of Inorganic Chemistry
Research Group for Catalysis and Solid State Chemistry II
Faculty of Chemistry
Gronostajowa 2, room. C2-20
30-381 Kraków
Poland
phone: +48 12 686 2471
makowski (at) chemia.uj.edu.pl
Teaching
Research
Selected publications
Polish version
Teaching
chemistry students | Principles of chemistry (lectures, laboratory, tutorials and calculus classes)
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PhD and masters theses
| Characterisation of adsorptive properties of zeolites and mesoporous materials
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Participation in projects
| IRRESISTIBLE: - project aimed at designing activities that foster the involvement of students and the public in the process of Responsible Research and Innovation (7th Framework Programme EU, nr 612367).
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Research
Scientific profile: | Porosity, adsorption, heterogeneous catalysis, thermal analysis
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Scientific interests: | Studies of porous structure and surface of adsorbents and catalysts by means of termodesorption techniques.
Adsorption of hydrocarbons and other organic compounds on porous adsorbents.
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Selected publications
2020
- A. Korzeniowska, W. Strzempek, W. Makowski, E. Menaszek. W.J. Roth, B. Gil
Incorporation and release of a model drug, ciprofloxacin, from non-modified SBA-15 molecular sieves with different pore sizes
Microporous and Mesoporous Materials, (2020)
doi: 10.1016/j.micromeso.2019.109903
2019
- A. Sławek, J. M. Vicent-Luna, K. Ogorzały, S. Valencia, F. Rey, W. Makowski, S. Calero
Adsorption of Alkanes in Zeolites LTA and FAU: Quasi-Equilibrated Thermodesorption Supported by Molecular Simulations
Journal of Physical Chemistry C, 123 (2019) 49
doi: 110.1021/acs.jpcc.9b07907
2018
- A. Sławek, K.Grzybowska, J.M. Vicent-Luna, W. Makowski, S. Calero
Adsorption of Cyclohexane in Pure Silica Zeolites: High-Throughput Computational Screening Validated by Experimental Data
ChemPhysChem, 19 (2018) 3364-3371
doi: 10.1002/cphc.201800968
- A. Sławek, J.M. Vicent-Luna, B. Marszałek, B. Gil, R.E. Morris, W. Makowski, S. Calero
Gate-Opening Mechanism of Hydrophilic-Hydrophobic Metal-Organic Frameworks: Molecular Simulations and Quasi-Equilibrated Desorption
Chemistry of Materials, 30 (2018) 5116-5127
doi: 10.1021/acs.chemmater.8b01603
- K. Roztocki, M. Lupa, A. Sławek, W. Makowski, I. Senkovska, S. Kaskel, D. Matoga
Water-Stable Metal-Organic Framework with Three Hydrogen-Bond Acceptors: Versatile Theoretical and Experimental Insights into Adsorption Ability and Thermo-Hydrolytic Stability
Inorganic Chemistry, 57 (2018) 3287-3296
doi: 10.1021/acs.inorgchem.8b00078
- W.J. Roth, B. Gil, A. Mayoral, J. Grzybek, A. Korzeniowska, M. Kubu, W. Makowski, J. Cejka, Z. Olejniczak, M. Mazur
Pillaring of layered zeolite precursors with ferrierite topology leading to unusual molecular sieves on the micro/mesoporous border
Dalton Transactions, 2018
doi: 10.1039/C7DT03718J
- D. Majda, T. Ikonen, A. Krupa, V.-P. Lehto, W. Makowski
Application of thermoporometry for characterization of mesoporous silicon: In search for probe liquid aimed at large pores
Microporous and Mesoporous Materials, 264 (2018) 1-7
doi: 10.1016/j.micromeso.2017.12.028
2017
- A. Sławek, J.M. Vicent-Luna, B. Marszałek, W. Makowski, S. Calero
Ordering of n-Alkanes Adsorbed in the Micropores of AlPO4-5: a Combined Molecular Simulations and Quasi-Equilibrated Thermodesorption Study
Journal of Physical Chemistry C, 121 (2017) 25292-25302
doi: 10.1021/acs.jpcc.7b08927
- A. Sławek, J.M. Vicent-Luna, B. Marszałek, W. Makowski, S. Calero
Quasi-Equilibrated Thermodesorption Combined with Molecular Simulation for Adsorption and Separation of Hexane Isomers in Zeolites MFI and MEL
Journal of Physical Chemistry C, 121 (2017) 19226-19238
doi: 10.1021/acs.jpcc.7b05347
2016
- A. Sławek, J.M. Vicent-Luna, B. Marszałek, S.R.G. Balestra, W. Makowski, S. Calero
Adsorption of n-Alkanes in MFI and MEL: Quasi-Equilibrated Thermodesorption Combined with Molecular Simulations
Journal of Physical Chemistry C, 120 (2016) 25338-25350
doi: 10.1021/acs.jpcc.6b06957
- D. Majda, B.D. Napruszewska, M. Zimowska, W. Makowski
Porosity of SBA-15 after functionalization of the surface with aminosilanes
Microporous and Mesoporous Materials, 234 (2016) 98-106
doi:10.1016/j.micromeso.2016.07.013
- W.J. Roth, B. Gil, W. Makowski, A. Sławek, J. Grzybek, M. Kubu, J. Cejka
Interconversion of the CDO layered precursor ZSM-55 between FER and CDO frameworks by controlled deswelling and reassembly
Chemistry of Materials, 28 (2016) 3616-3619
doi: 10.1021/acs.chemmater.6b01302
- W.J. Roth, B. Gil, W. Makowski, A. Sławek, A. Korzeniowska, J. Grzybek, M. Siwek, P. Michorczyk
Framework-substituted cerium MCM-22 zeolite and its interlayer expanded derivative MWW-IEZ
Catalysis Science & Technology, 6 (2016) 2742-2753
doi: 10.1039/C5CY02074C
- W.J. Roth, B. Gil, W. Makowski, B. Marszalek, P. Eliásová
Layer like porous materials with hierarchical structure
Chemical Society Reviews, 45 (2016) 3400-3438
doi: 10.1039/C5CS00508F
- K.A. Tarach, J. Tekla, W. Makowski, U. Filek, K. Mlekodaj, V. Girman, M. Choi, K. Góra-Marek
Catalytic dehydration of ethanol over hierarchical ZSM-5 zeolites: studies of their acidity and porosity properties
Catalysis Science & Technology, 6 (2016) 3568-3584
doi: 10.1039/C5CY01866H
- D. Majda, A. Korzeniowska, W. Makowski, A. Michalik-Zym, B.D. Napruszewska, M. Zimowska, E.M. Serwicka
Thermoporosimetry of n-alkanes for characterization of mesoporous SBA-15 silicas - refinement of methodology
Microporous and Mesoporous Materials, 222 (2016) 33-43
doi:10.1016/j.micromeso.2015.10.002
2015
- A. Pacuła, P. Nowak, W. Makowski, R. Socha
The influence of layered double hydroxide composition on the morphology, porosity and capacitive properties of nitrogen-doped carbon materials prepared via chemical vapor deposition
Microporous and Mesoporous Materials, 201 (2015) 1-9
doi: 10.1016/j.micromeso.2014.09.006
- D. Majda, W. Makowski, M. Mańko, K. Mlekodaj, A. Michalik-Zym, B.D. Napruszewska, M. Zimowska, E.M. Serwicka
Porosity characterization of SBA-15 silicas with thermoporosimetry of water and n-alkanes - the effect of the probe liquid nature
Microporous and Mesoporous Materials, 201 (2015) 141-150
doi: 10.1016/j.micromeso.2014.09.021
- B. Gil, W.J. Roth, W. Makowski, B. Marszalek, D. Majda, Z. Olejniczak, P. Michorczyk
Facile evaluation of the crystallization and quality of the transient layered zeolite MCM-56 by infrared spectroscopy
Catalysis Today, 243 (2015) 39-45
doi: 10.1016/j.cattod.2014.07.031
2014
- W.J. Roth, W. Makowski, B. Marszalek, P. Michorczyk, W. Skuza, B. Gil
Activity enhancement of zeolite MCM-22 by interlayer expansion enabling higher Ce loading and room temperature CO oxidation
Journal of Materials Chemistry A, 38 (2014) 15722-15725
doi: 10.1039/C4TA03308F
- M. Inger, M. Wilk, M. Saramok, G. Grzybek, A. Grodzka, P. Stelmachowski, W. Makowski, A. Kotarba, Z. Sojka
Cobalt spinel catalyst for N2O abatement in the pilot plant operation – long term activity and stability in tail gases
Industrial & Engineering Chemistry Research, 53 (2014) 10335-10342
doi: 10.1021/ie5014579
- W. Makowski, M. Mańko, P. Zabierowski, K. Mlekodaj, D. Majda, J. Szklarzewicz, W. Łasocha
Unusual adsorption behavior of volatile hydrocarbons on MOF-5 studied using thermodesorption methods
Thermochimica Acta, 587 (2014) 1-10
doi: 10.1016/j.tca.2014.04.016
- W. Makowski, K. Mlekodaj, B. Gil, W.J Roth, B. Marszalek, M. Kubu, P. Hudec, A. Smieskova, M. Hornacek
Application of quasi-equilibrated thermodesorption of linear and di-branched paraffin molecules for detailed porosity characterization of mono-layered zeolite MCM-56, in comparison to MCM-22 and ZSM-5
Dalton Transactions, 43 (2014) 10574-10583
doi: 10.1039/C4DT00232F
- B. Gil, W. Makowski, B. Marszalek, W.J. Roth, M. Kubu, J. Cejka and Z. Olejniczak
High acidity unilamellar zeolite MCM-56 and its pillared and delaminated derivatives
Dalton Transactions, 43 (2014)10501-10511
doi: 10.1039/C4DT00130C
- K. Tarach, K. Góra-Marek, J. Tekla, K. Brylewska, J. Datka, K. Mlekodaj, W. Makowski, M.C. Igualada López, J. Martínez Triguero, F. Rey
Catalytic cracking performance of alkaline-treated zeolite Beta in the terms of acid sites properties and their accessibility
Journal of Catalysis, 312 (2014) 46-57
doi: 10.1016/j.jcat.2014.01.009
- K. Mlekodaj, K. Sadowska, J. Datka, K. Góra-Marek, W. Makowski
Porosity and accessibility of acid sites in desilicated ZSM-5 zeolites studied using adsorption of probe molecules,
Microporous and Mesoporous Materials, 183 (2014) 54-61
doi: 10.1016/j.micromeso.2013.08.051
2013
- W. Makowski, K. Mlekodaj, D. Majda,
Characterization of acidic zeolite catalysts by thermodesorption and cracking of n-nonane
Microporous and Mesoporous Materials, 166 (2013) 137-143
doi: /10.1016/j.micromeso.2012.04.034
- M. Mańko, R. Chal, P. Trens, D. Minoux, C. Gérardin, W. Makowski
Porosity of micro-mesoporous zeolites prepared via pseudomorphic transformation of zeolite Y crystals: a combined isothermal sorption and thermodesorption investigation
Microporous and Mesoporous Materials, 170 (2013) 243
doi: 10.1016/j.micromeso.2012.12.016
- W. Makowski, M. Mańko, A. Dudek, K. Mlekodaj,
Application of quasi-equilibrated thermodesorption of hexane and cyclohexane for characterization of porosity of zeolites and ordered mesoporous silicas
Adsorption, 19 (2013) 537-544
doi: 10.1007/s10450-013-9476-9
- M. Mańko, J. Vittenet, J. Rodriguez, D. Cot, J. Mendret, S. Brosillon, W. Makowski, A. Galarneau
Synthesis of binderless zeolite aggregates (SOD, LTA, FAU) beads of 10, 70 μm and 1 mm by direct pseudomorphic transformation
Microporous and Mesoporous Materials, 176 (2013) 145–154
doi: 0.1016/j.micromeso.2013.04.006
2012
- D. Majda, W. Makowski, M. Mańko,
Pore size distribution of micelle-templated silicas studied by thermoporosimetry using water and n-heptane,
Journal of Thermal Analysis and Calorimetry, 109 (2012) 663-669
doi: 10.1007/s10973-012-2372-9
2010
- W. Makowski, M. Leżańska, M. Mańko, J. Włoch
Porosity and surface properties of mesoporous silicas and their carbon replicas investigated with quasi-equlibrated thermodesorption of n-hexane and n-nonane
Journal of Porous Materials, 17 (2010) 737-745
doi: 10.1007/s10934-009-9345-9
- D. Majda, W. Makowski,
Studies on the equilibrated thermodesorption of n-hexane from ZSM-5 zeolite - The influence of the extraframework cations
Journal of Thermal Analysis and Calorimetry, 101 (2010) 519-526
doi: 10.1007/s10973-010-0832-7
- M. Mańko, B. Gil, R. Janus, P. Ku¶trowski, W. Makowski
Characterization of the porosity and surface chemistry of mesoporous silicas by quasi-equilibrated thermodesorption of 1-butanol and n-nonane
Thermochimica Acta, 511 (2010) 82-88
doi:10.1016/j.tca.2010.07.028
2009
- W. Makowski, L. Chmielarz, P. Ku¶trowski
Determination of the pore size distribution of mesoporous silicas by means of quasi-equilibrated thermodesorption of n-nonane
Microporous and Mesoporous Materials, 120 (2009) 257-262
doi: 10.1016/j.micromeso.2008.11.014
2008
- W. Makowski, B. Gil, D. Majda
Characterization of acidity and porosity of zeolite catalysts by the equilibrated thermodesorption of n-hexane and n-nonane
Catalysis Letters, 120 (2008) 154-160
doi: 10.1007/s10562-007-9268-5
2007
- W. Makowski, D. Majda
Temperature programmed desorption of n-hexane and n-heptane from MFI and FAU zeolites
Journal of Porous Materials, 14 (2007) 27
doi: 10.1007/s10934-006-9004-3
- W. Makowski
Quasi equilibrated temperature programmed desorption and adsorption - a new method for determination of the isosteric adsorption heat
Thermochimica Acta, 454 (2007) 26-32
doi: 10.1016/j.tca.2006.12.015
- W. Makowski, P. Ku¶trowski
Probing pore structure of microporous and mesoporous molecular sieves by quasi-equilibrated temperature programmed desorption and adsorption of n-nonane
Microporous and Mesoporous Materials, 102 (2007) 283-289
doi: 10.1016/j.micromeso.2007.01.009
- W. Makowski, Ł. Ogorzałek
Determination of the adsorption heat of n-hexane and n-heptane on zeolites beta, L, 5A, 13X, Y and ZSM-5 by means of quasi equilibrated temperature programmed desorption and adsorption (QE-TPDA)
Thermochimica Acta, 465 (2007) 30-39
doi: 10.1016/j.tca.2007.09.002
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