dr hab. Wacław Makowski

Zespół Katalizy Heterogenicznej
i Fizykochemii Ciała Stałego II

Wydział Chemii UJ
ul. Ingardena 3, p. 136
30-060 Kraków

tel. (012) 6632245
makowski (at) chemia.uj.edu.pl


Badania
Dydaktyka
Wybrane publikacje

English version


Badania

Specjalno¶ć: Adsorpcja, kataliza heterogeniczna, analiza termiczna

Zainteresowania naukowe: Badania struktury porowatej oraz powierzchni adsorbentów i katalizatorów metodami termodesorpcyjnymi.

Badania adsorpcji węglowodorów i innych zwi±zków organicznych na adsorbentach porowatych.


Dydaktyka

I rok chemiiPodstawy chemii
(wykłady, konwersatoria i ćwiczenia rachunkowe)

Prace magisterskie i doktorskie
Tematyka: badania wła¶ciwo¶ci adsorpcyjnych zeolitów i materiałów mezoporowatych
kandydaci mile widziani!


Wybrane publikacje

2014

  1. M. Inger, M. Wilk, M. Saramok, G. Grzybek, A. Grodzka, P. Stelmachowski, W. Makowski, A. Kotarba, Z. Sojka
    Cobalt spinel catalyst for N2O abatement in the pilot plant operation – long term activity and stability in tail gases
    Industrial & Engineering Chemistry Research, 53 (2014) 10335-10342
    doi: 10.1021/ie5014579

  2. W. Makowski, M. Mańko, P. Zabierowski, K. Mlekodaj, D. Majda, J. Szklarzewicz, W. Łasocha
    Unusual adsorption behavior of volatile hydrocarbons on MOF-5 studied using thermodesorption methods
    Thermochimica Acta, 587 (2014) 1-10
    doi: 10.1016/j.tca.2014.04.016

  3. W. Makowski, K. Mlekodaj, B. Gil, W.J Roth, B. Marszalek, M. Kubu, P. Hudec, A. Smieskova, M. Hornacek
    Application of quasi-equilibrated thermodesorption of linear and di-branched paraffin molecules for detailed porosity characterization of mono-layered zeolite MCM-56, in comparison to MCM-22 and ZSM-5
    Dalton Transactions, 43 (2014) 10574-10583
    doi: 10.1039/C4DT00232F

  4. B. Gil, W. Makowski, B. Marszalek, W.J. Roth, M. Kubu, J. Cejka and Z. Olejniczak
    High acidity unilamellar zeolite MCM-56 and its pillared and delaminated derivatives
    Dalton Transactions, 43 (2014)10501-10511
    doi: 10.1039/C4DT00130C

  5. K. Tarach, K. Góra-Marek, J. Tekla, K. Brylewska, J. Datka, K. Mlekodaj, W. Makowski, M.C. Igualada López, J. Martínez Triguero, F. Rey
    Catalytic cracking performance of alkaline-treated zeolite Beta in the terms of acid sites properties and their accessibility
    Journal of Catalysis, 312 (2014) 46-57
    doi: 10.1016/j.jcat.2014.01.009

  6. K. Mlekodaj, K. Sadowska, J. Datka, K. Góra-Marek, W. Makowski
    Porosity and accessibility of acid sites in desilicated ZSM-5 zeolites studied using adsorption of probe molecules,
    Microporous and Mesoporous Materials, 183 (2014) 54-61
    doi: 10.1016/j.micromeso.2013.08.051

2013

  1. W. Makowski, K. Mlekodaj, D. Majda,
    Characterization of acidic zeolite catalysts by thermodesorption and cracking of n-nonane
    Microporous and Mesoporous Materials, 166 (2013) 137-143
    doi: /10.1016/j.micromeso.2012.04.034

  2. M. Mańko, R. Chal, P. Trens, D. Minoux, C. Gérardin, W. Makowski
    Porosity of micro-mesoporous zeolites prepared via pseudomorphic transformation of zeolite Y crystals: a combined isothermal sorption and thermodesorption investigation
    Microporous and Mesoporous Materials, 170 (2013) 243
    doi: 10.1016/j.micromeso.2012.12.016

  3. W. Makowski, M. Mańko, A. Dudek, K. Mlekodaj,
    Application of quasi-equilibrated thermodesorption of hexane and cyclohexane for characterization of porosity of zeolites and ordered mesoporous silicas
    Adsorption, 19 (2013) 537-544
    doi: 10.1007/s10450-013-9476-9

  4. M. Mańko, J. Vittenet, J. Rodriguez, D. Cot, J. Mendret, S. Brosillon, W. Makowski, A. Galarneau
    Synthesis of binderless zeolite aggregates (SOD, LTA, FAU) beads of 10, 70 μm and 1 mm by direct pseudomorphic transformation
    Microporous and Mesoporous Materials, 176 (2013) 145–154
    doi: 0.1016/j.micromeso.2013.04.006

2012

  1. D. Majda, W. Makowski, M. Mańko,
    Pore size distribution of micelle-templated silicas studied by thermoporosimetry using water and n-heptane,
    Journal of Thermal Analysis and Calorimetry, 109 (2012) 663-669
    doi: 10.1007/s10973-012-2372-9

2010

  1. W. Makowski, M. Leżańska, M. Mańko, J. Włoch
    Porosity and surface properties of mesoporous silicas and their carbon replicas investigated with quasi-equlibrated thermodesorption of n-hexane and n-nonane
    Journal of Porous Materials, 17 (2010) 737-745
    doi: 10.1007/s10934-009-9345-9

  2. D. Majda, W. Makowski,
    Studies on the equilibrated thermodesorption of n-hexane from ZSM-5 zeolite - The influence of the extraframework cations
    Journal of Thermal Analysis and Calorimetry, 101 (2010) 519-526
    doi: 10.1007/s10973-010-0832-7

  3. M. Mańko, B. Gil, R. Janus, P. Ku¶trowski, W. Makowski
    Characterization of the porosity and surface chemistry of mesoporous silicas by quasi-equilibrated thermodesorption of 1-butanol and n-nonane
    Thermochimica Acta, 511 (2010) 82-88
    doi:10.1016/j.tca.2010.07.028

2009

  1. W. Makowski, L. Chmielarz, P. Ku¶trowski
    Determination of the pore size distribution of mesoporous silicas by means of quasi-equilibrated thermodesorption of n-nonane
    Microporous and Mesoporous Materials, 120 (2009) 257-262
    doi: 10.1016/j.micromeso.2008.11.014

2008

  1. W. Makowski, B. Gil, D. Majda
    Characterization of acidity and porosity of zeolite catalysts by the equilibrated thermodesorption of n-hexane and n-nonane
    Catalysis Letters, 120 (2008) 154-160
    doi: 10.1007/s10562-007-9268-5

2007

  1. W. Makowski, D. Majda
    Temperature programmed desorption of n-hexane and n-heptane from MFI and FAU zeolites
    Journal of Porous Materials, 14 (2007) 27
    doi: 10.1007/s10934-006-9004-3

  2. W. Makowski
    Quasi equilibrated temperature programmed desorption and adsorption - a new method for determination of the isosteric adsorption heat
    Thermochimica Acta, 454 (2007) 26-32
    doi: 10.1016/j.tca.2006.12.015

  3. W. Makowski, P. Ku¶trowski
    Probing pore structure of microporous and mesoporous molecular sieves by quasi-equilibrated temperature programmed desorption and adsorption of n-nonane
    Microporous and Mesoporous Materials, 102 (2007) 283-289
    doi: 10.1016/j.micromeso.2007.01.009

  4. W. Makowski, Ł. Ogorzałek
    Determination of the adsorption heat of n-hexane and n-heptane on zeolites beta, L, 5A, 13X, Y and ZSM-5 by means of quasi equilibrated temperature programmed desorption and adsorption (QE-TPDA)
    Thermochimica Acta, 465 (2007) 30-39
    doi: 10.1016/j.tca.2007.09.002